標題: | Growth of N-Glycyl-L-Valine (GV) single crystal and its spectral, thermal and optical characterization |
作者: | Janarthanan, S. Samuel, R. Sugaraj Rajan, Y. C. Suresh, P. Thangaraj, K. 材料科學與工程學系 Department of Materials Science and Engineering |
關鍵字: | Crystal growth;X-ray techniques;Thermal analysis |
公開日期: | 15-Mar-2013 |
摘要: | A nonlinear optical crystal of N-Glycyl-L-Valine (GV) single crystals was grown by slow evaporation solution growth technique from an aqueous solution. The unit cell parameters and the crystal structure were determined by single crystal X-ray diffraction study. The Fourier transform infrared (FTIR) and proton nuclear magnetic resonance (H-1 NMR) spectral studies were carried out to identify the functional groups of the grown crystals. The ultraviolet visible near infrared (UV-Vis-NIR) spectrum was recorded to study the optical transparency of the grown crystal. The thermogravimetric (TG) and differential thermal (DTA) analyses revealed the thermal stability of the sample. The presence of second harmonic generation (SHG) for the grown crystal was confirmed by Kurtz-Perry powder technique. (C) 2012 Elsevier B.V. All rights reserved. |
URI: | http://dx.doi.org/10.1016/j.saa.2012.10.078 http://hdl.handle.net/11536/21731 |
ISSN: | 1386-1425 |
DOI: | 10.1016/j.saa.2012.10.078 |
期刊: | SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY |
Volume: | 105 |
Issue: | |
起始頁: | 34 |
結束頁: | 37 |
Appears in Collections: | Articles |
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